Sr. No.
|
NAME OF RAW MATERIALS |
PARAMETERS SPECIFIED |
REQUIREMENTS |
1
|
H-Acid M.W. =319 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Grayish moist material/Dry powder
- 55%-65% for moist material
- 78-80% for dry powder
- 0.20% Max.
- Clear solution in dilute alkali
- Chromotropic acid 1% Max.
- Koch acid 0.3% Max
- Omega acid 0.3% Max.
- All other impurities <1.5% Max.
|
2
|
J. Acid M. W =239 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Material/Dry powder
- 88%-90% By coupling value Min.
- 0.20% Max.
- Soluble in dilute alkali
- Iso Amino G.0.20* Max.
- Di j. Acid 0.5% Max.
- All other impurities <1.0% Max.
|
3
|
Cyanuric Chloride M. W=184.5 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- White crystalline powder Highly
- lacrymatic
- 98% Min.
- 0.1% in Benzene
- Clear Solution in Benzene
- Nil
|
4 |
Sodium Naphthionate (free acid0 M.W=223) |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Pinkish moist/dry material
- 70% Min.
- 0.2% Max.
- Soluble in dilute alkali
- Naphthyl amine 0.1% Ma.
- Others 0.2% Max.
|
5 |
DASDSA M.W =370 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Yellow moist/dry material
- 65% for moist material
- 90% for dry material
- 0.2% Max.
- Soluble in dilute alkali
- Di – hydro product 1% Max.
|
6 |
BDSA M.W.=344 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Yellowish moist material
- 65% Min
- 0.2% Max
- Clear solution in dilute alkali
- Metanilic acid 0.5% Max
|
7 |
Tobias Acid M.W =223 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Light pinkish dry powder
- 98% Min.
- 0.2% Max
- Soluble in dilute alkali
|
8 |
2-pyridone M.W.=196 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Plate yellow dry powder
- 95% Min
- 0.2% Max
- Soluble in dilute alkali
- 1% Max all together
|
9 |
Vinyl Sulfone M.W=311 (ortho anisidine base) |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Off white to light gray dry powder
- 90% Min
- 0.5% Max.
- Soluble in water
- Difference between Diazo value and hydrolysis value 4% Max.
|
10 |
Vinyl Sulfone
M.W.=341 2,5-Di
Methoxy aniline base |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Grayish dry powder
- 85% Min
- 0.8% Max
- Soluble in water
- Difference between Diazo value and
- hydrolysis value 3% Max.
|
11 |
Vinyl Sulfone
M.W.=325
(para cresidine) |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Grayish dry powder
- 90% Min
- 0.5% Max
- Soluble in dilute alkali forming clear solution with bluish fluorescence.
- Amino G. 0.3% Max
|
12 |
K-Acid M.W=383 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Yellowish moist material
- 65% Min
- 0.2% Max
- Soluble in dilute alkali forming clear solution with bluish fluorescence
- 1.0% Max all together
|
13 |
C-Acid M.W.=303 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Pinkish moist/dry material
- 65% Min for moist material
- 80% Min for dry material
- 0.20% Max
- Clear solution in dilute alkali with bluish 1.0% Max all together
|
14 |
Meta Ureido Anline
M.W.=151 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Pinkish dry powder
- 70% Min.
- 0.2% Max
- Clear solution in hot dilute acid
- 2% max Di Ureido product
|
15 |
Metanilic Acid M.W.=173 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- White to light pinkish dry powder
- 98% Min.
- 0.2% Max.
- Clear Solution dilute alkali
- Nil
|
16 |
Orthanlic Acid M.W=173 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- White to cream colored dry powder
- 98% Min
- 0.2% Max.
- Clear solution in dilute alkali
- Nil
|
17 |
5 – Sulfo Anthanilic
Acid M.W = 217 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Pale yellow dry powder
- 95% Min
- 0.2% Max.
- Clear solution in dilute alkali
- Anthranilic acid Nil
- Paper Chromatogram – single spot
|
18 |
Metaphenylene Diamine M.W=108 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Blackish crystalline material
- 95% Min
- 0.2% Max
- Clear solution water.
- Nil
|
19 |
Beta Naphthol
M.W.=144 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Off-white thin-small flakes
- 98% min set point 121 C
- o.1% Max
- Soluble in dilute Caustic Soda
- 1 – Naphthol 0.3% Max.
|
20 |
Para Phenylene diamine (PPD) M.W.=108 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- White to off-white crystalline powder or lumps.
- 99% Min.
- 0.1% Max.
- Soluble in water and dilute acid
- PNA <0.1%
- Ash content 0.1%
- Melting point 139 – 141 C
|
21 |
MPDSA M.W = 188 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Pinkish crystalline material
- 70% Min. sodium salt
- 98% Min. free acid
- 0.2% Max
- Sodium salt soluble in water freely
- Free acid soluble in dilute alkali
- Single spot on Paper Chromatogram.
|
22 |
MPDSA M.W = 268 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Brownish dry material
- 80% Min
- 0.2% Max
- Soluble in dilute alkali
- 2% Max all impurities
|
23 |
Gamma Acid
M.W.=239 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
Gray dry powder
- 90% Min by coupling values.
- 0.20% Max
- Clear solution in dilute alkali
- 1. Amino G.0.2% Max
- 2. Dioxy Compound 0.3% Max
- Bronner’s acid 1.0% Max
- All other impurities <1.0%
|
24 |
N -Methyl J – Acid
M.W.=253 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Brownish moist/dry material
- 75% moist material 85% Min dry powder
- 0.20% Max
- Soluble in dilute alkali
- Unreacted J-Acid 3% Max
- Di J – Acid 0.5% max.
|
25 |
Sulfo Tobias Acid
M.W.=303 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Light pinkish moist material
- 65% Min
- 0.2% Max
- Clear solution in dilute alkali
- Unreacted Tobias Acid – Nil
- 2- Napthyl amine 5- Sulfonic acid – Nil
|
26 |
Vinyl sulfone
(para base)
M.W =281 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Off white dry powder
- 95% Min
- 0.5% Max.
- Soluble in water
- Difference between Diazo value and Hydrolysis value -1.55 Max.
|
27 |
Bromamine Acid
M.W.=382 |
- Appearance
- Assay
- Insoluble
- Solubility
- Impurities
|
- Bright red powder
- 90% Min
- 0.2% Max
- Soluble in hot dilute alkali
- 1% Max. Unbrominated product.
|